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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66410-27-3
合成路线
（共 29 条）
66410-27-3
→
反应条件
53120-27-7
(3Z,13Z)-3,13-十八碳二烯-1-基乙酸酯
反应条件
1: H2, quinoline / Pd-BaSO4 / hexane 2: 98 percent / NaOAc / 0 °C View Scheme
参考文献
Singh, Vasundhara; Trehan, I. R.; Kad, G. L.
Journal of the Indian Chemical Society, 1992 , vol. 69, # 2 p. 103 - 105
250328-13-3
→
反应条件
66410-27-3
反应条件
disodium hydrogenphosphate; sodium amalgam in methanol T=20°C; 21 h;
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
67616-77-7
→
反应条件
66410-27-3
反应条件
pyridinium p-toluenesulfonate in methanol T=55°C; 6 h;
参考文献
Trehan, I R; Kad, G L; Singh, Vasundhara; Vig, Rakesh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 6 p. 563 - 566
59499-29-5
→
反应条件
66410-27-3
反应条件
1: 81 percent / dimethylformamide / 4 h / 110 °C 2: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 3: 84 percent / p-TsOH / methanol / 16 h / 20 °C 4: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
250328-09-7
→
反应条件
66410-27-3
反应条件
1: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 2: 84 percent / p-TsOH / methanol / 16 h / 20 °C 3: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
250328-17-7
→
反应条件
66410-27-3
反应条件
1: 82 percent / NaI / acetone / 48 h / Heating 2: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 3: 84 percent / p-TsOH / methanol / 16 h / 20 °C 4: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
250328-11-1
→
反应条件
66410-27-3
反应条件
1: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 2: 84 percent / p-TsOH / methanol / 16 h / 20 °C 3: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
250328-12-2
→
反应条件
66410-27-3
反应条件
1: 84 percent / p-TsOH / methanol / 16 h / 20 °C 2: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
60274-60-4
1-氯-5-碘戊烷
→
反应条件
66410-27-3
反应条件
1.1: BuLi / tetrahydrofuran / 0.5 h / 20 °C 1.2: 33 percent / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / 20 °C 2.1: 82 percent / NaI / acetone / 48 h / Heating 3.1: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 4.1: 84 percent / p-TsOH / methanol / 16 h / 20 °C 5.1: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
59499-28-4
(4Z)-4-壬烯基-1-醇
→
反应条件
66410-27-3
反应条件
1: tetrahydrofuran / 0.33 h / 20 °C 2: LiBr / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Heating 3: 81 percent / dimethylformamide / 4 h / 110 °C 4: 66 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / -78 - -50 °C 5: 84 percent / p-TsOH / methanol / 16 h / 20 °C 6: 97 percent / Na(Hg); Na2HPO4 / methanol / 21 h / 20 °C View Scheme
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848
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