Armitage, Mark; Bret, Guillaume; Choudary, Bernie M.; Kingswood, Mike; Loft, Mike; Moore, Steve; Smith, Steve; Urquhart, Michael W. J.
Organic Process Research and Development, 2012 , vol. 16, # 10 p. 1626 - 1634
sulfuric acid; hydrogen; platinum(IV) oxide in methanol
T=20°C; 18 h;
参考文献
Armitage, Mark; Bret, Guillaume; Choudary, Bernie M.; Kingswood, Mike; Loft, Mike; Moore, Steve; Smith, Steve; Urquhart, Michael W. J.
Organic Process Research and Development, 2012 , vol. 16, # 10 p. 1626 - 1634
1: H2; H2SO4 / PtO2 / methanol / 18 h / 20 °C
2: HNO3; AcOH / 2 h / 20 °C
3: Et3N; H2O / tetrahydrofuran / 18 h / 20 °C
4: K2CO3 / acetone / 18 h / Heating
5: H2 / Pd/C / 18 h / 50 °C / 2250.18 Torr
6: HCl / diethyl ether; propan-2-ol / 18 h / Heating
7: i-Pr2NEt / propan-2-ol / 48 h / Heating
View Scheme
参考文献
Armitage, Mark; Bret, Guillaume; Choudary, Bernie M.; Kingswood, Mike; Loft, Mike; Moore, Steve; Smith, Steve; Urquhart, Michael W. J.
Organic Process Research and Development, 2012 , vol. 16, # 10 p. 1626 - 1634
