4-氯-2,6-二(5-氯-2-羟基苯基)甲基-苯酚合成路线 （共 7 条）
反应条件
zinc(II) chloride
0.0111111 h; microwave irradiation;
参考文献
Khalafi-Nezhad, Ali; Rad, Mohammad Navid Soltani; Hakimelahi, Gholam Hossein
Helvetica Chimica Acta, 2003 , vol. 86, # 7 p. 2396 - 2403
反应条件
sulfuric acid in methanol; water
T=-5 - 0°C; 2 h;
参考文献
Hakimelahi, Gholam Hosein; Moshfegh, Ali Akbar
Helvetica Chimica Acta, 1981 , vol. 64, # 2 p. 599 - 609
反应条件
1: 80 percent / 25percent aq. NaOH / methanol / 1.) 60-80 deg C, 1 h; 2.) RT, 24 h
2: 78 percent / conc. HCl / methanol / 12 h / Ambient temperature
View Scheme
参考文献
Moshfegh, Ali Akbar; Mazandarani, Behnaz; Nahid, Azarmidokht; Hakimelahi, Gholam Hosein
Helvetica Chimica Acta, 1982 , vol. 65, # 4 p. 1229 - 1232
反应条件
1: aq. HCl
View Scheme
参考文献
Rodia,J.S.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2966 - 2969
参考文献
Rodia,J.S.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2966 - 2969
反应条件
methanol; sodium hydroxide
参考文献
Zinke; Hanus
Chemische Berichte, 1941 , vol. 74, p. 205,211
参考文献
Zinke; Hanus
Chemische Berichte, 1941 , vol. 74, p. 205,211
