4-硝基-1,8-萘醛酸酐合成路线 (共 25 条)
反应条件
sodium dichromate in acetic acid 5 h; Reflux;
参考文献
Dong, Ming; Wang, Ya-Wen; Peng, Yu
Organic Letters, 2010 , vol. 12, # 22 p. 5310 - 5313
反应条件
sodium dichromate in acetic acid 10 h; Heating;
参考文献
Solodar', S. L.; Kochkin, V. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 10 p. 1820 - 1823
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 10 p. 2137 - 2141
反应条件
sodium dichromate; acetic acid T=22 - 25°C; 5 h;
参考文献
Dubey, Krishna K.; Singh, Ramendra K.; Misra, Krishna
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 10 p. 876 - 878
反应条件
1: HNO3; AcOH 2: Na2Cr2O7; H2SO4 View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 54, # 4 p. 1021 - 1028
反应条件
1: 95 percent / acetic acid / 2 h / Ambient temperature 2: 87 percent / conc. H2SO4, HNO3 / 2 h / 1.) 0 to 2 deg C, 1 h, 2.) room temp., 1 h. 3: 78 percent / sodium bichromate / acetic acid / 10 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, # 10 p. 1820 - 1823
Zhurnal Organicheskoi Khimii, , vol. 16, # 10 p. 2137 - 2141
反应条件
1: 87 percent / conc. H2SO4, HNO3 / 2 h / 1.) 0 to 2 deg C, 1 h, 2.) room temp., 1 h. 2: 78 percent / sodium bichromate / acetic acid / 10 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, # 10 p. 1820 - 1823
Zhurnal Organicheskoi Khimii, , vol. 16, # 10 p. 2137 - 2141
反应条件
1: 57 percent / HNO3, CH3COOH 2: 78 percent / Na2Cr2O7, AcOH / 5 h / 22 - 25 °C View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 34, # 10 p. 876 - 878
反应条件
beim Aufbewahren im Vakuum ueber Schwefelsaeure; beim Erhitzen oder beim Behandeln mit Eisessig;
参考文献
Chemische Berichte, , vol. 21, p. 1460
反应条件
1: tin (II)-chloride; aqueous hydrochloric acid 2: aqueous HCl View Scheme
参考文献
Okazaki; Ishikawa
Yuki Gosei Kagaku Kyokaishi, 1956 , vol. 14, p. 398,400
Chem.Abstr., 1957 , p. 8051
反应条件
ammonia in ethanol 48 h; sealed tube;
参考文献
Alexiou, Michael; Tyman, John; Wilson, Ian
Tetrahedron Letters, 1981 , vol. 22, # 24 p. 2303 - 2306