triethylamine; 1-(toluene-p-sulphonyl)imidazole in N,N-dimethyl-formamide
Reflux;
参考文献
Rad, Mohammad Navid Soltani; Behrouz, Somayeh; Nekoei, Abdo-Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2014 , vol. 189, # 4 p. 465 - 476
1.1: hydrogenchloride; sodium nitrite / water / 0.17 h / -5 °C
1.2: 1.75 h / -5 - 0 °C
2.1: tetrahydrofuran / 0.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Rennison, David; Conole, Daniel; Tingle, Malcolm D.; Yang, Junpeng; Eason, Charles T.; Brimble, Margaret A.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6629 - 6635
