1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran T=-20°C; 0.25 h; 2: With LiH3BNMe2 in tetrahydrofuran T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
1: iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride / tetrahydrofuran / 0.25 h / -20 °C 2: LiH3BNMe2 / tetrahydrofuran / 16 h / -20 - 20 °C View Scheme
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran
T=-20°C; 0.25 h;
2: With LiH3BNMe2 in tetrahydrofuran
T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
