3-溴-1-丙烯膦酸二乙酯合成路线 （共 5 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 1.5 h; Heating;
参考文献
Hashimoto, Masashi; Hemmi, Keiji; Takeno, Hidekazu; Kamiya, Takashi
Tetrahedron Letters, 1980 , vol. 21, p. 99 - 102
反应条件
pyridine; phosphorus tribromide in dichloromethane 12 h; Heating;
参考文献
Poss, A. J.; Smyth, M. S.
Synthetic Communications, 1987 , vol. 17, # 14 p. 1735 - 1740
反应条件
1: 67 percent / Br2 / CCl4 / 5 h / 20 °C 2: 63 percent / TBAF; K2CO3 / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 69, # 7 p. 1088 - 1092
反应条件
tetrabutyl ammonium fluoride; potassium carbonate in tetrahydrofuran Dehydrobromination; 4 h; Heating;
参考文献
Rozhko; Ragulin
Russian Journal of General Chemistry, 1999 , vol. 69, # 7 p. 1088 - 1092
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in diethyl ether 2 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 9 p. 2251 - 2253
