1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride in chloroform 2 h; Heatingother trimethylsilyl enolates; var. solvents, temperatures and reaction time; Product distribution;
参考文献
Ohta, Shunsaku; Yamashita, Masayuki; Nagai, Nobuaki; Kawasaki, Ikuo; Maeda, Kazuto; Miyano, Yoshiko
Heterocycles, 1995 , vol. 41, # 8 p. 1683 - 1690
反应条件
water; cesium fluoride 1.) 40 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Boyer, J.; Corriu, R. J. P.; Perz, R.; Reye, C.
Journal of Organometallic Chemistry, 1980 , vol. 184, # 2 p. 157 - 166
反应条件
potassium tert-butylate
参考文献
Katritzky, Alan R.; Hayden, Amy E.; Kirichenko, Kostyantyn; Pelphrey, Phillip; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5108 - 5111
反应条件
titanium(III)-tris-(tetrahydridoborate) in dichloromethane T=-20°C; 1 h;
参考文献
Ravikumar; Chandrasekaran, Srinivasan
Tetrahedron, 1997 , vol. 53, # 8 p. 2973 - 2978
反应条件
1: With dimethylsulfide borane complex in tetrahydrofuran T=0 - 20°C; 2: With benzene-1,2-diol; triethylamine in tetrahydrofuran T=0 - 20°C; 3: With oxygen in tetrahydrofuran T=20°C; 12 h; Further stages.;
参考文献
Cadot, Christine; Dalko, Peter I.; Cossy, Janine; Ollivier, Cyril; Chuard, Rachel; Renaud, Philippe
Journal of Organic Chemistry, 2002 , vol. 67, # 21 p. 7193 - 7202
反应条件
in water; acetonitrile T=80°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 43, # 33 p. 5751 - 5753
参考文献
Blaney; Grigg; Rankovic; Thoroughgood
Tetrahedron Letters, 2000 , vol. 41, # 34 p. 6639 - 6642
反应条件
indium(III) chloride in water T=23°C; 15 h;
参考文献
Loh, Teck-Peng; Pei, Jian; Cao, Guo-Qiang
Chemical Communications, 1996 , # 15 p. 1819 - 1820
反应条件
1.1: Ce(NH4)2(NO3)6; CaCO3 / ethanol / cooling 1.2: 62 percent / aq. H2SO4 / dioxane / 5 h / 20 °C 2.1: 83 percent / aq. NH4OH / ethanol / 150 °C View Scheme
参考文献
Azzuz, A.; Sorokin, V. L.; Kulinkovich, O. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 1 p. 31 - 33
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 1 p. 37 - 39
反应条件
2: diethyl ether / 3 h / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 26 p. 3239 - 3242
