1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
参考文献
Blaney; Grigg; Rankovic; Thoroughgood
Tetrahedron Letters, 2000 , vol. 41, # 34 p. 6639 - 6642
反应条件
potassium tert-butylate
参考文献
Katritzky, Alan R.; Hayden, Amy E.; Kirichenko, Kostyantyn; Pelphrey, Phillip; Ji, Yu
Journal of Organic Chemistry, 2004 , vol. 69, # 15 p. 5108 - 5111
反应条件
lithium carbonate; diphenyldisulfane in dimethyl sulfoxide T=40°C; 6 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.
Journal of Organic Chemistry, 1993 , vol. 58, # 10 p. 2678 - 2685
反应条件
1: 1-(trimethylsilyloxy)-1-cyclohexene With methyllithium in diethyl ether T=0°C; 0.5 h; 2: With gallium(III) chloride in diethyl ether; hexane T=0 - 20°C; 0.5 h; 3: phenacyl iodine With air; triethyl borane in diethyl ether; hexane T=25°C; 0.5 h;
参考文献
Usugi, Shin-ichi; Yorimitsu, Hideki; Shinokubo, Hiroshi; Oshima, Koichiro
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 9 p. 2049 - 2052
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
参考文献
Zhdankin, Viktor V.; Tykwinski, Rik; Caple, Roland; Berglund, Bruce; Koz'min, Anatoly S.; Zefirov, Nikolai S.
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3703 - 3704
反应条件
in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Zhdankin, Viktor V.; Mullikin, Michelle; Tykwinski, Rik; Berglund, Bruce; Caple, Ronald; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2605 - 2608
反应条件
in benzene 22 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
in benzene 22 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
(CF3CH2O)VOCl2 T=-78°C; 0.5 h;
参考文献
Ryter; Livinghouse
Journal of the American Chemical Society, 1998 , vol. 120, # 11 p. 2658 - 2659