1-(三甲基硅氧烷)环己烯合成路线 (共 370 条)
反应条件
titanium(IV) isopropylate; titanium tetrachloride in dichloromethane -90 deg C, 90 min;
参考文献
Mateos, A. Fernandez; Fuente Blanco, Jesus A. de la
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1349 - 1354
反应条件
tert.-butylhydroperoxide; MoVIO2(acetylacetone)2 in benzene T=60°C; 48 h;
参考文献
Tetrahedron Letters, , vol. 22, # 27 p. 2595 - 2598
反应条件
tert.-butylhydroperoxide; titanium silicate 24 h; Heating;
参考文献
Chemical Communications, , # 16 p. 1969 - 1970
反应条件
in acetonitrile 1 h; Irradiation; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 2742 - 2751
反应条件
tris-(dibenzylideneacetone)dipalladium(0); Bu3SnF; tri-tert-butyl phosphine in toluene
24 h; Inert atmosphereReflux;
参考文献
Cheon, Cheol Hong; Kanno, Osamu; Toste, F. Dean
Journal of the American Chemical Society, 2011 , vol. 133, # 34 p. 13248 - 13251
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene
19 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
tri-tert-butyl phosphine; tri-n-butyltin fluoride; tris(dibenzylideneacetone)dipalladium (0) in benzene
20 h; Heating;
参考文献
Iwama, Tetsuo; Rawal, Viresh H.
Organic Letters, 2006 , vol. 8, # 25 p. 5725 - 5728
反应条件
trimethylsilyl iodide in acetonitrile
T=20°C; 1 h;
参考文献
Kozyukov, V. P.; Kozyukov, Vik. P.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 2 p. 467 - 468,414 - 415
反应条件
α-cyclohexylcyclohexanemethanamine; trimethylsilyl iodide in acetonitrile
13 h; Ambient temperature;
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 547 - 550
反应条件
in acetonitrile
T=0°C; Yield given;
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668