1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
in benzene
22 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
in benzene
22 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
反应条件
[Rh(I)(cycloocta-1,5-diene)(butane-1,4-diylbis[diphenylphosphine])]ClO4 in dichloromethane
T=100°C; 42 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Izumi, Yusuke
Journal of Organometallic Chemistry, 1988 , vol. 352, p. 223 - 238
反应条件
bis-(trifluoromethylsulphonyl)amine in dichloromethane
T=-78°C; 2 h; optical yield given as percent dediastereoselective reaction;
参考文献
Kurahashi, Kei; Takemoto, Yoshiji; Takasu, Kiyosei
ChemSusChem, 2012 , vol. 5, # 2 p. 270 - 273
反应条件
trimethylsilyl trifluoromethanesulfonate; triethylamine in dichloromethane
19 h; Ambient temperature;
参考文献
Duthaler; Wegmann
Helvetica Chimica Acta, 1984 , vol. 67, # 7 p. 1755 - 1766
反应条件
1: 1.) TiCl4 / 1.) dichloromethane, -78 deg C, 30 min, 2.) dichloromethane, -50 deg C, 18 h
2: sodium hydride / tetrahydrofuran / 2 h / Ambient temperature
View Scheme
参考文献
Duhamel, Pierre; Poirier, Jean-Marie; Tavel, Gilbert
Tetrahedron Letters, 1984 , vol. 25, # 1 p. 43 - 46
反应条件
sodium methylate; di-n-butylbis(trifluoromethanesulfonyloxy)stannane
1) CH2Cl2, 5h, -78 deg C 2) MeOH, 3h, room temperature; Yield given. Multistep reaction;
参考文献
Sato, Tsuneo; Wakahara, Yoshiyuki; Otera, Junzo; Nozaki, Hitosi
Tetrahedron Letters, 1990 , vol. 31, # 11 p. 1581 - 1584
反应条件
sodium methylate; di-n-butylbis(trifluoromethanesulfonyloxy)stannane
1) CH2Cl2, -78 deg C, 5h, 2) MeOH, 3h, RT; Yield given. Multistep reaction;
参考文献
Sato, Tsuneo; Wakahara, Yoshiyuki; Otera, Junzo; Nozaki, Hitosi
Tetrahedron, 1991 , vol. 47, # 47 p. 9773 - 9782
反应条件
hydrogenchloride in tetrahydrofuran
0.5 h; Ambient temperature; Yield given;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
1: 78 percent Chromat. / CH2Cl2 / 5 h / Ambient temperature
2: 81 percent / boron trifluoride etherate / 5 h / Ambient temperature
View Scheme
参考文献
Rubottom, George M.; Mott, Robert C.; Juve, Henrik D.
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2717 - 2721
