1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
hydrogenchloride; di-n-butylbis(trifluoromethanesulfonyloxy)stannane
other silyl enol ethers;
参考文献
Sato, Tsuneo; Wakahara, Yoshiyuki; Otera, Junzo; Nozaki, Hitosi
Tetrahedron Letters, 1990 , vol. 31, # 11 p. 1581 - 1584
反应条件
in water
T=60°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Lubineau, Andre; Meyer, Elsa
Tetrahedron, 1988 , vol. 44, # 19 p. 6065 - 6070
反应条件
aluminum oxide; zinc(II) chloride in tetrahydrofuran
T=0 - 5°C; 1.5 h;
参考文献
Ranu, Brindaban C.; Saha, Manika; Bhar, Sanjay
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 15 p. 2197 - 2200
反应条件
TASF-(Et) in tetrahydrofuran
T=-78°C; 2 h;
参考文献
Noyori, R.; Nishida, I.; Sakata, J.
Journal of the American Chemical Society, 1983 , vol. 105, # 6 p. 1598 - 1608
反应条件
1: 75 percent / copper(II)-pentandionate / benzene / 90 °C
2: 83 percent / (C2H5)3NHF / tetrahydrofuran / 1 h / 25 °C
View Scheme
参考文献
Fleming, Ian; Iqbal, Javed
Tetrahedron Letters, 1983 , vol. 24, # 3 p. 327 - 328
反应条件
potassium tert-butylate
1.) THF, -20 deg C, 45 min, 2.) -15 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Quesnel, Yannick; Bidois-Sery, Laure; Poirier, Jean-Marie; Duhamel, Lucette
Synlett, 1998 , # 4 p. 413 - 415
反应条件
caesium carbonate in dichloromethane
24 h; Ambient temperature;
参考文献
Barani, Marco; Fioravanti, Stefania; Pellacani, Lucio; Tardella, Paolo A.
Tetrahedron, 1994 , vol. 50, # 38 p. 11235 - 11238
参考文献
Lociuro, Sergio; Pellacani, Lucio; Tardella, Paolo A.
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 593 - 596
反应条件
CaO in dichloromethane
3.5 h; Ambient temperaturevarious solid inorganic bases were used; Product distribution;
参考文献
Barani, Marco; Fioravanti, Stefania; Antonietta Loreto; Pellacani, Lucio; Tardella, Paolo A.
Tetrahedron, 1994 , vol. 50, # 12 p. 3829 - 3834
反应条件
tris(pentafluorophenyl)-borane; hydrogen; dppn in benzene
T=20°C; P=1500.15 Torr; 20 h;
参考文献
Wang, Huadong; Froehlich, Roland; Kehr, Gerald; Erker, Gerhard
Chemical Communications, 2008 , # 45 p. 5966 - 5968
