1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
Cu(MeCN)ClO4 in acetonitrile
T=-20°C;
参考文献
Evans, David A.; Faul, Margaret M.; Bilodeau, Mark T.
Journal of the American Chemical Society, 1994 , vol. 116, # 7 p. 2742 - 2753
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 0.2 h; Inert atmosphere;
参考文献
Yoshimura, Akira; Nemykin, Victor N.; Zhdankin, Viktor V.
Chemistry - A European Journal, 2011 , vol. 17, # 38 p. 10538 - 10541
反应条件
[Ru(1,4,7-trimethyl-1,4,7-triazacyclononane)Cl3]; silver perchlorate
1.) MeOH, r.t., 3 h, 2.) CH3CN, r.t., 3 h; Yield givenMultistep reaction;
参考文献
Au, Sze-Man; Zhang, Suo-Bo; Fung, Wai-Hong; Yu, Wing-Yiu; Che, Chi-Ming; Cheung, Kung-Kai
Chemical Communications, 1998 , # 24 p. 2677 - 2678
反应条件
bis-(trifluoromethylsulphonyl)amine in dichloromethane
T=-78°C; Mukaiyama cross-aldol reaction; 2 h;
参考文献
Cossy; Lutz; Alauze; Meyer
Synlett, 2002 , # 1 p. 45 - 48
反应条件
2,6-di-tert-butyl-pyridine; trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=16°C; 10 h;
参考文献
Murata, S.; Suzuki, M.; Noyori, R.
Tetrahedron Letters, 1980 , vol. 21, p. 2527 - 2528
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Heating;
参考文献
Hayashi, Tamio; Katsuro, Yoshio; Kumada, Makoto
Tetrahedron Letters, 1980 , vol. 21, p. 3915 - 3918
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-n-butyltin fluoride; triethylamine; [(t-Bu)3PH]BF4 in benzene
T=80°C; 24 h; Inert atmosphere;
参考文献
Beck, Elizabeth M.; Hyde, Alan M.; Jacobsen, Eric N.
Organic Letters, 2011 , vol. 13, # 16 p. 4260 - 4263
反应条件
in 1,2,2-trifluoro-trichloroethane
T=40°C; 3 h; in degassed and sealed tube;
参考文献
Yoshida, Masato; Moriya, Koji; Sawada, Hideo; Kobayashi, Michio
Chemistry Letters, 1985 , p. 755 - 758
反应条件
1: I2 / CH2Cl2
2: CH2Cl2
3: Et3N*HF / CH2Cl2 / 2 h
View Scheme
参考文献
Rubottom, George M.; Mott, Robert C.; Juve, Henrik D.
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2717 - 2721
反应条件
copper(l) chloride in various solvent(s)
27 h; Ambient temperature;
参考文献
Ito, Hajime; Ishizuka, Tomoko; Tateiwa, Jun-Ichi; Hosomi, Akira
Tetrahedron Letters, 1998 , vol. 39, # 35 p. 6295 - 6298
