1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
1: CH2Cl2 2: aq. HCl View Scheme
参考文献
Danishefsky; Kitahara; McKee; Schuda
Journal of the American Chemical Society, 1976 , vol. 98, # 21 p. 6715 - 6717
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prieto, J. Antonio; Larson, Gerald L.
Synthetic Communications, 1980 , vol. 10, # 9 p. 675 - 684
反应条件
1: 84 percent / Et3N / tetrahydrofuran / 1 h / Heating; Irradiation 2: 96 percent / KF / acetone / 1 h / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 119, # 2 p. 444 - 452
反应条件
potassium fluoride; tri-n-butyl-tin hydride 1.) THF, irradiation, 30 min, 2.) acetone, 1 h; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 119, # 2 p. 444 - 452
反应条件
[Rh(H)(PEt3)3]; tributylphosphine in 1,4-dioxane T=100°C; 2 h;
参考文献
Tsuji, Jiro; Minami, Ichiro; Shimizu, Isao
Tetrahedron Letters, 1984 , vol. 25, # 45 p. 5157 - 5160
反应条件
[VO(OEt)Cl2] in dichloromethane T=-75°C;
参考文献
Tetrahedron, , vol. 50, # 34 p. 10207 - 10214
反应条件
tetrakis(triphenylphosphine) palladium(0); n-butyllithium 1.) THF, hexane, -78 deg C, 2.) THF, hexane, a) -78 deg C, 1 h, b) RT, overnight; Yield given. Multistep reaction;
参考文献
Hirao, Toshikazu; Yamada, Naoto; Ohshiro, Yoshiki; Agawa, Toshio
Journal of Organometallic Chemistry, 1982 , vol. 236, # 3 p. 409 - 414
反应条件
trimethylsilyl trifluoromethanesulfonate; iodosylbenzene Ambient temperature1.) CH2Cl2, 2.) CH2Cl2, RT, overnight; Yield given;
参考文献
Moriarty, Robert M.; Epa, Widanagamage R.; Prakash, Om
Journal of Chemical Research - Part S, 1997 , # 7 p. 262 - 263
反应条件
TASF-(Et) in tetrahydrofuran T=-78°C; 3 h;
参考文献
Noyori, R.; Nishida, I.; Sakata, J.
Journal of the American Chemical Society, 1983 , vol. 105, # 6 p. 1598 - 1608
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Prieto, J. Antonio; Larson, Gerald L.
Synthetic Communications, 1980 , vol. 10, # 9 p. 675 - 684
