1-(三甲基硅氧烷)环己烯合成路线 （共 370 条）
反应条件
boron trifluoride diethyl etherate in diethyl ether; dichloromethane T=0 - 20°C;
参考文献
Sydnes, Leiv K.; Pedersen, Gry S.; Holmelid, Bjarte; Sandberg, Marcel
Synthesis, 2007 , # 23 p. 3692 - 3696
反应条件
boron trifluoride diethyl etherate in diethyl ether; dichloromethane T=0 - 20°C;
参考文献
Sydnes, Leiv K.; Pedersen, Gry S.; Holmelid, Bjarte; Sandberg, Marcel
Synthesis, 2007 , # 23 p. 3692 - 3696
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; tri-n-butyltin fluoride in benzene T=20 - 60°C; 24 h; Inert atmosphere;
参考文献
Cheon, Cheol Hong; Imahori, Tatsushi; Yamamoto, Hisashi
Chemical Communications, 2010 , vol. 46, # 37 p. 6980 - 6982
反应条件
samarium (III) iodide in tetrahydrofuran T=80°C; 4 h;
参考文献
Bao, Weiliang; Zhang, Yongmin; Ying, Taokai
Synthetic Communications, 1996 , vol. 26, # 3 p. 503 - 507
反应条件
phosphorus pentachloride in benzene Heating;
参考文献
Lazukina,L.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1976 , vol. 46, # 9 p. 2006 - 2011,1931 - 1935
反应条件
water; (S, S)-6,6’-bis(1-hydroxy-2,2-dimethylpropyl)-2,2’-bipyridine; scandium tris(trifluoromethanesulfonate) in acetonitrile T=-20°C; 34 h; Title compound not separated from byproducts;
参考文献
Ishikawa, Shunpei; Hamada, Tomoaki; Manabe, Kei; Kobayashi, Shu
Journal of the American Chemical Society, 2004 , vol. 126, # 39 p. 12236 - 12237
反应条件
P(o-tol)3 gold(I) chloro complex; silver trifluoromethanesulfonate in 1,4-dioxane T=100°C; 10 h;
参考文献
Aikawa, Haruo; Kaneko, Tetsuro; Asao, Naoki; Yamamoto, Yoshinori
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, art. no. 76, p. 648 - 652
反应条件
PPh3 gold(I) chloro complex; silver perchlorate in benzene T=80°C; 2 h;
参考文献
Aikawa, Haruo; Kaneko, Tetsuro; Asao, Naoki; Yamamoto, Yoshinori
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, art. no. 76, p. 648 - 652
反应条件
zinc(II) chloride in dichloromethane T=0°C; 1 h; further reagent: ZnBr2;
参考文献
Reetz, Manfred T.; Walz, Peter; Huebner, Friedhelm; Huettenhain, Stefan H.; Heimbach, Horst; Schwellnus, Konrad
Chemische Berichte, 1984 , vol. 117, # 1 p. 322 - 335
反应条件
zinc(II) chloride in dichloromethane Ambient temperatureovernight; further reagents: ZnI2, ZnBr2;
参考文献
Reetz, Manfred T.; Walz, Peter; Huebner, Friedhelm; Huettenhain, Stefan H.; Heimbach, Horst; Schwellnus, Konrad
Chemische Berichte, 1984 , vol. 117, # 1 p. 322 - 335
