1-(三甲硅烷氧基)-1,3-丁二烯合成路线 （共 23 条）
反应条件
triethylamine; zinc(II) chloride in benzene
参考文献
Jung, Michael E.; Gardiner, John M.
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2614 - 2615
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Jung, Michael E.; Castro, Claire; Gardiner, John M.
Tetrahedron Letters, 1991 , vol. 32, # 41 p. 5717 - 5720
反应条件
palladium diacetate; methyl-ethyl phosphite in tetrahydrofuran Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 10 p. 1641 - 1644
反应条件
1: 82 percent / SO3*pyridine, Et3N, DMSO / CH2Cl2 / 2 h / Ambient temperature 2: 1.) sodium tert-amylate / 1.) benzene, reflux, 2.) benzene, reflux to RT 3: Pd(OAc)2, triisopropylphosphite / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 52, # 21 p. 7487 - 7510
反应条件
triethylamine; zinc(II) chloride T=85 - 90°C; 24 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 1001 - 1003
Zhurnal Organicheskoi Khimii, , vol. 18, # 6 p. 1159 - 1162
参考文献
Tetrahedron Letters, , vol. 22, # 29 p. 2833 - 2836
反应条件
hydrogenchloride; hydroquinone 1) 130 deg C, 7 h, sealed tube; 2) 95-100 deg C, 1 h.; Yield given. Multistep reaction;
参考文献
Makin, S. M.; Tung, Nguyen Fyong; Shavrygina, O. A.; Arshava, B. M.; Romanova, I. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 4 p. 640 - 645
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 4 p. 727 - 732
反应条件
T=60°C; Diels-Alder reaction; 24 h; Ionic liquidSealed ampoule;
参考文献
Rosa, Claudia Della; Ormachea, Carla; Kneeteman, Maria N.; Adam, Claudia; Mancini, Pedro M.E.
Tetrahedron Letters, 2011 , vol. 52, # 50 p. 6754 - 6757
反应条件
T=60°C; Diels-Alder reaction; 24 h; Ionic liquidSealed ampoule;
参考文献
Rosa, Claudia Della; Ormachea, Carla; Kneeteman, Maria N.; Adam, Claudia; Mancini, Pedro M.E.
Tetrahedron Letters, 2011 , vol. 52, # 50 p. 6754 - 6757
反应条件
N-bromosuccinmide in tetrahydrofuran; methanol T=-20 - 20°C; 1.5 h;
参考文献
Girard, Anne-Lise; Lhermet, Rudy; Fressigne, Catherine; Durandetti, Muriel; Maddaluno, Jacques
European Journal of Organic Chemistry, 2012 , # 15 p. 2895 - 2905
反应条件
bromine 1) DMF, -20 deg C; Yield given. Multistep reaction;
参考文献
Gaonac'h, Odile; Maddaluno, Jacques; Chauvin, Joe; Duhamel, Lucette
Journal of Organic Chemistry, 1991 , vol. 56, # 12 p. 4045 - 4048
