3,4,5-三苯基-2(3H)-恶唑酮合成路线 （共 9 条）
反应条件
2C17H14O*Pd(2+); potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=70°C; 8 h; Inert atmosphere;
参考文献
Lu, Zenghui; Cui, Weijian; Xia, Siyuan; Bai, Yihui; Luo, Fang; Zhu, Gangguo
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9871 - 9877,7
反应条件
lithium chloride in N,N-dimethyl-formamide
T=60°C; 0.5 h;
参考文献
Siegel, Hannes; Wittmann, Helga
Monatshefte fuer Chemie, 1982 , vol. 113, p. 1005 - 1018
反应条件
T=130°C; 24 h; Inert atmosphereNeat (no solvent);
参考文献
Santoyo, Blanca M.; Gonzalez-Romero, Carlos; Merino, Omar; Martinez-Palou, Rafael; Fuentes-Benites, Aydee; Jimenez-Vazquez, Hugo A.; Delgado, Francisco; Tamariz, Joaquin
European Journal of Organic Chemistry, 2009 , # 15 p. 2505 - 2518
反应条件
in toluene
6 h; Heating;
参考文献
Sakai, Shizuyoshi; Murata, Masashi; Wada, Nobuto; Fujinami, Tatsuo
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1873 - 1874
反应条件
ammonia
T=210 - 220°C; im Rohr;
参考文献
McCombie; Parkes
Journal of the Chemical Society, 1912 , vol. 101, p. 1997
参考文献
v. Auwers; Mauss
Biochemische Zeitschrift, 1928 , vol. 192, p. 222
反应条件
sodium
1) ether, reflux, 4 h; 2) ether.; Yield given. Multistep reaction;
参考文献
Mehrotra, Kailash Nath; Singh, Indra Sen; Roy, Jalpana
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 8 p. 2399 - 2402
反应条件
1: sodium bicarbonate
2: alcoholic KOH-solution
View Scheme
参考文献
McCombie; Parkes
Journal of the Chemical Society, 1912 , vol. 101, p. 1997
反应条件
pyridine; N,N-dimethyl-formamide
参考文献
Gompper
Chemische Berichte, 1956 , vol. 89, p. 1762,1767
