3-二甲基氨基-1,2-双(4-甲氧基苯基)-2-丙烯-1-酮合成路线 (共 5 条)
反应条件
in N,N-dimethyl-formamide T=140°C; 2 h;
参考文献
Klose; Schwarz
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 5 p. 1165 - 1167
反应条件
in N,N-dimethyl-formamide Condensation; 18 h; Heating;
参考文献
Gupton, John T.; Krumpe, Keith E.; Burnham, Bruce S.; Webb, Tammy M.; Shuford, Jordan S.; Sikorski, James A.
Tetrahedron, 1999 , vol. 55, # 51 p. 14515 - 14522
反应条件
1: With trichlorophosphate in dichloromethane Substitution; 5 h; Heating; 2: With water in tetrahydrofuran T=25°C; Hydrolysis; Title compound not separated from byproducts;
参考文献
Burnham; Gupton; Krumpe; Webb; Shuford; Bowers; Warren; Barnes; Hall
Archiv der Pharmazie, 1998 , vol. 331, # 11 p. 337 - 341
反应条件
1: With trichlorophosphate in dichloromethane Substitution; 5 h; Heating; 2: With water in tetrahydrofuran T=25°C; Hydrolysis; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 55, # 51 p. 14515 - 14522
反应条件
sodium in ethanol
5 h; Heating;
参考文献
Klose; Schwarz
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 5 p. 1165 - 1167