4 - (吡啶-2基)嘧啶-2-胺合成路线 （共 6 条）
反应条件
sodium in ethanol 16 h; Heating;
参考文献
Bejan; Ait Haddou; Daran; Balavoine
Synthesis, 1996 , # 8 p. 1012 - 1018
反应条件
sodium in ethanol 24 h; Inert atmosphereReflux;
参考文献
Taghizadeh Ghoochany, Leila; Kerner, Christian; Farsadpour, Saeid; Menges, Fabian; Sun, Yu; Niedner-Schatteburg, Gereon; Thiel, Werner R.
European Journal of Inorganic Chemistry, 2013 , # 24 p. 4305 - 4317
反应条件
sodium ethanolate in ethanol T=65°C; 4 h;
参考文献
Yu, Xian-Yong; Yi, Ping-Gui; Ji, Dan-Hong; Zeng, Bi-Rong; Li, Xiao-Fang; Xu, Xin
Dalton Transactions, 2012 , vol. 41, # 13 p. 3684 - 3694
反应条件
1: 1 h / 110 °C 2: sodium ethanolate / ethanol / 4 h / 65 °C View Scheme
参考文献
Dalton Transactions, , vol. 41, # 13 p. 3684 - 3694
反应条件
sodium in ethanol 12 h; RefluxSchlenk technique;
参考文献
Dalton Transactions, , vol. 43, # 6 p. 2397 - 2405
反应条件
1: copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine / 1,4-dioxane / 20 h / 20 - 100 °C / |Inert atmosphere; |Schlenk technique
2: hydrazine hydrate; anhydrous iron chloride; carbon / water / 80 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Liu, Yi-Feng; Wang, Cui-Ling; Bai, Ya-Jun; Han, Ning; Jiao, Jun-Ping; Qi, Xiao-Li
Organic Process Research and Development, 2008 , vol. 12, # 3 p. 490 - 495
