双[2-(二苯基膦基)乙基]胺盐酸盐合成路线 (共 3 条)
反应条件
hydrogenchloride; potassium tert-butylate in tetrahydrofuran
16 h; Heating;
参考文献
Nuzzo, Ralph G.; Haynie, Sharon L.; Wilson, Michael E.; Whitesides, George M.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2861 - 2867
反应条件
(trimethyl)silylmethyllithium in diethyl ether
T=20°C; 24 h; Inert atmosphere;
参考文献
Zhang, Guoqi; Vasudevan, Kalyan V.; Scott, Brian L.; Hanson, Susan K.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8668 - 8681
反应条件
triethylamine in N,N-dimethyl-formamide
60 h; Ambient temperature;
参考文献
Nuzzo, Ralph G.; Haynie, Sharon L.; Wilson, Michael E.; Whitesides, George M.
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2861 - 2867