反应条件
in n-heptane
stirring overnight at ambient temp., then for 6 h at 60°C;; removal the volatiles under reduced pressure, distn. in vac., elem. anal.;;
参考文献
Bai, J.; Niedenzu, K.; Serwatowska, J.; Serwatowski, J.
Inorganic Chemistry, 1991 , vol. 30, p. 4631 - 4635