2: Na(Hg), MeOH / tetrahydrofuran / 8 h / -20 °C 3: aq. KOH / ethanol / 1 h / Heating 4: thionyl chloride / 1.) RT, 18 h, 2.) 100 deg C, 30 min View Scheme
参考文献
Gannett, Peter M.; Nagel, Donald L.; Reilly, Pam J.; Lawson, Terence; Sharpe, Jody; Toth, Bela
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 1064 - 1071
1: With ammonia in methanol; water T=35°C; P=22502.3 Torr; 0.00416667 h; 2: With hydrogen; 5 ruthenium on Al2O3 in methanol; water T=120°C; P=22502.3 Torr; 22 h;
参考文献
DSM N.V.; Du Pont de Nemours and Company
Patent: US6353100 B1, 2002 ;
Location in patent: Page column 11,12 ;
