1: 4-(trifluoromethyl)-2-nitroaniline With phosphoric acid in water
T=50°C; 1.25 h;
2: With sodium nitrite in water
T=0°C; 0.75 h;
3: β-naphthol in methanol; water
T=0°C; 0.416667 h; Cooling with ice;
参考文献
CIBA HOLDING INC.
Patent: WO2008/101842 A1, 2008 ;
Location in patent: Page/Page column 37 ;