2,3-二甲基-1,2-丁二醇合成路线 （共 12 条）
反应条件
potassium permanganate; sodium carbonate
参考文献
Criegee
Justus Liebigs Annalen der Chemie, 1930 , vol. 481, p. 263,286
Chemische Berichte, 1931 , vol. 64, p. 260,264
反应条件
potassium permanganate; water
参考文献
Delacre
Chem. Zentralbl., 1906 , vol. 77, # II p. 498
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Couturier
Annales de Chimie (Cachan, France), 1892 , vol. <6>26, p. 476
反应条件
1: sodium disulfite; water
2: hydrogen chloride / anschliessendes Behandeln mit Wasser
3: copper oxide-chromium oxide; ethanol / 200 °C / 257428 Torr / Hydrogenation
View Scheme
参考文献
Green; Hickinbottom
Journal of the Chemical Society, 1957 , p. 3270,3272
反应条件
ethanol; copper oxide-chromium oxide
T=200°C; P=257428 Torr; Hydrogenation;
参考文献
Green; Hickinbottom
Journal of the Chemical Society, 1957 , p. 3270,3272
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Sheehan,J.C.; Howell,M.G.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2279 - 2282
反应条件
1: aq. NaOH
2: LiAlH4 / diethyl ether
View Scheme
参考文献
Sheehan,J.C.; Howell,M.G.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2279 - 2282
反应条件
1: alcoholic KOH-solution
2: water; KMnO4
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参考文献
Couturier
Annales de Chimie (Cachan, France), 1892 , vol. <6>26, p. 476
反应条件
1: aqueous sulfuric acid
2: sodium disulfite; water
3: hydrogen chloride / anschliessendes Behandeln mit Wasser
4: copper oxide-chromium oxide; ethanol / 200 °C / 257428 Torr / Hydrogenation
View Scheme
参考文献
Green; Hickinbottom
Journal of the Chemical Society, 1957 , p. 3270,3272
反应条件
1: hydrogen chloride / anschliessendes Behandeln mit Wasser
2: copper oxide-chromium oxide; ethanol / 200 °C / 257428 Torr / Hydrogenation
View Scheme
参考文献
Green; Hickinbottom
Journal of the Chemical Society, 1957 , p. 3270,3272
反应条件
Hydrogenation; 2.3-dimethyl-butene-(1)-diol-(3.4) substance of Criegee;
参考文献
Criegee
Justus Liebigs Annalen der Chemie, 1930 , vol. 483, p. 304
Full Text Show Details
Criegee
Justus Liebigs Annalen der Chemie, 1930 , vol. 481, p. 263,286
Chemische Berichte, 1931 , vol. 64, p. 260,264
