N-(4-氯苯基)-2-溴苯甲酰胺合成路线 (共 4 条)
反应条件
triethylamine in ethyl acetate
T=0 - 20°C; 1 h;
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672
反应条件
triethylamine in dichloromethane
T=20°C; 2 h;
参考文献
Liu, Bifu; Li, Yibiao; Jiang, Huanfeng; Yin, Meizhou; Huang, Huawen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2288 - 2300
反应条件
copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in N,N-dimethyl-formamide
T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
1.2: 2 h / 0 - 20 °C / Inert atmosphere
2.1: di-μ-chlorobis [5-hydroxy-2-[1-(hydroxyimino)ethyl]phenyl]palladium(II) dimer; potassium carbonate / N,N-dimethyl acetamide / 72 h / 140 °C / Inert atmosphere
View Scheme
参考文献
Zhang, Guofu; Zhao, Xiaobao; Yan, Yunbing; Ding, Chengrong
European Journal of Organic Chemistry, 2012 , # 4 p. 669 - 672