1: 72 percent / butyllithium / tetrahydrofuran; hexane / -100 °C
2: 77 percent / magnesium bromide-diethyl ether / diethyl ether / 48 h / Ambient temperature
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3103 - 3112
MgBr2(Et2O) in tetrahydrofuran
72 h; Heating; Yield given;
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3103 - 3112
MgBr2(Et2O) in diethyl ether
48 h; Ambient temperature;
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3103 - 3112
