N-Boc-L-苯丙氨醇合成路线 (共 89 条)
反应条件
sodium tetrahydroborate; acetic acid in 1,4-dioxane; methanol
参考文献
Synlett, , # 18 art. no. G24405ST, p. 2802 - 2804
反应条件
sodium tetrahydroborate in methanol
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 17, # 6 p. 1788 - 1792
反应条件
1: 70 percent / Raney-Nickel; AcOH; hydrogen / methanol / 16 h / 20 °C / 3102.97 Torr 2: 0.1 g / triethylamine / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1: 1) HCl, 2) aq. Na2CO3 / 2) CHCl3 2: 80 percent / NaBH4, LiI / tetrahydrofuran / 8 h / Heating View Scheme
参考文献
Synlett, , vol. 1997, # 2 p. 171 - 172
反应条件
sodium tetrahydroborate
参考文献
Organic letters, , vol. 3, # 6 p. 897 - 899
反应条件
1.1: C54H53NO2Si2; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; dibenzoyl peroxide / dichloromethane / 20 h / 0 °C 1.2: 0.5 h / 20 °C 2.1: 5 palladium on charcoal; hydrogen / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 48 p. 18036 - 18039
反应条件
1.1: sodium hydrogencarbonate / tetrahydrofuran; methanol / 60 h 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 60 h / 20 °C / Cooling with ice 2.2: 0.58 h / 0 - 20 °C View Scheme
反应条件
sodium; ammonium chloride in ammonia
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 639 - 640
反应条件
sodium; ammonium chloride in ammonia
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 639 - 640
反应条件
lithium aluminium tetrahydride Reduction;
参考文献
Synlett, , # 11 p. 1631 - 1633