N-Boc-L-苯丙氨醇合成路线 （共 89 条）
反应条件
lithium aluminium tetrahydride 1.) THF, reflux, 7 h, 2.) THF, H2O, CH2Cl2, 60 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 54, # 51 p. 15673 - 15678
反应条件
2,4,6-trichloro-1,3,5-triazine; dimethyl sulfoxide; triethylamine in tetrahydrofuran T=-30 - 20°C; 2.5 h;
参考文献
De Luca; Giacomelli; Porcheddu
Journal of Organic Chemistry, 2001 , vol. 66, # 23 p. 7907 - 7909
反应条件
trifluoroacetic acid Substitution;
参考文献
Douat-Casassus, Celine; Pulka, Karolina; Claudon, Paul; Guichard, Gilles
Organic Letters, 2012 , vol. 14, # 12 p. 3130 - 3133
反应条件
pyridine in dichloromethane 12 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 14 p. 2505 - 2508
反应条件
pyridine in chloroform 22 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 40, # 13 p. 2629 - 2632
反应条件
1H-imidazole in N,N-dimethyl-formamide T=20°C;
参考文献
Kishore Kumar; Baskaran, Sundarababu
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4520 - 4523
反应条件
1: pyridine 2: pyridine 3: TFA / CH2Cl2 View Scheme
参考文献
Christoffers, Jens; Mann, Alexander
Angewandte Chemie - International Edition, 2000 , vol. 39, # 15 p. 2752 - 2754
反应条件
1: triethylamine / CH2Cl2 / 1 h / 0 °C 2: LiAlH4 / tetrahydrofuran / 4 h / Heating 3: 72 percent / anhydrous potassium carbonate / acetonitrile / 12 h / 25 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1: triethylamine / CH2Cl2 / 1 h / 0 °C 2: LiAlH4 / tetrahydrofuran / 4 h / Heating View Scheme
参考文献
Talluri, Siva Kumar; Sudalai, Arumugam
Tetrahedron, 2007 , vol. 63, # 39 p. 9758 - 9763
反应条件
1: pyridine / CHCl3 / 22 h 2: H2O2, NaOH / methanol; H2O / 2 h View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 13 p. 2629 - 2632
