4-丙基硫代-1,2-亚苯基二胺合成路线 （共 13 条）
反应条件
sodium dithionite in ethanol Heating;
参考文献
Hazelton; Iddon; Suschitzky; Woolley
Tetrahedron, 1995 , vol. 51, # 39 p. 10771 - 10794
反应条件
Saccharomyces cerevisiae; methanol; sodium hydroxide in water
参考文献
Blackie, Josie A.; Turner, Nicholas J.; Wells, Andrew S.
Tetrahedron Letters, 1997 , vol. 38, # 17 p. 3043 - 3046
反应条件
hydrogen; palladium on activated charcoal in ethanol T=25°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 21 p. 4615 - 4622
反应条件
1: 98.5 percent / NaOH / ethane-1,2-diol; H2O / 5 h / Heating 2: H2 / Pd/C / ethanol / 25 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 11, # 21 p. 4615 - 4622
反应条件
1.1: chlorine / methanol / 7 h / 10 °C / Industry scale 2.1: sodium hydroxide / water; propan-1-ol / 35 °C / Industry scale 3.1: water; propan-1-ol / 40 - 60 °C / Industry scale 3.2: 60 °C 4.1: NaSH / methanol / 50 - 70 °C / Industry scale View Scheme
反应条件
1.1: sodium hydroxide / water; propan-1-ol / 35 °C / Industry scale 2.1: water; propan-1-ol / 40 - 60 °C / Industry scale 2.2: 60 °C 3.1: NaSH / methanol / 50 - 70 °C / Industry scale View Scheme
反应条件
1: 60 percent / propan-1-ol / -10 - 0 °C 2: 74 percent / Na2S2O4 / aq. ethanol / Heating View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 99, # 9 p. 673 - 701
反应条件
1: 60 percent / propan-1-ol / -10 - 0 °C 2: 74 percent / Na2S2O4 / aq. ethanol / Heating View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 99, # 9 p. 673 - 701
反应条件
1: 4-(propylthio)-1,2-phenylenediamine With hydrogenchloride in water; acetone T=80 - 85°C; Industry scale; 2: sodium salt of cyanocarbamic acid methyl ester T=20 - 85°C; pH=4 - 4.5;
参考文献
SEQUENT SCIENTIFIC LIMITED; RANE, Ramkrishna Appaji; NAITHANI, Sushil; NATIKAR, Rajendra Devendra; VERMA, Sudhakar; ARULMOLI, Thangavel
Patent: WO2012/70069 A2, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
hydrogenchloride in water; acetone T=85°C; Large scale;
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Naithani, Sushil; Natikar, Rajendra Devendra; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303782 A1, 2013 ;
Location in patent: Paragraph 0031 ;
