4-(2,2-二乙氧基乙氧基)甲苯合成路线 (共 5 条)
反应条件
1: 77 percent / poly-phosphoric acid / benzene / 3.5 h / Heating 2: 35 percent / benzoyl peroxide; N-bromosuccinimide / CCl4 / 30 h / Heating View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
反应条件
potassium hydroxide in dimethyl sulfoxide
6 h; Heating;
参考文献
Barker, Peter; Finke, Paul; Thompson, Kevan
Synthetic Communications, 1989 , vol. 19, # 1, 2 p. 257 - 266
反应条件
sodium ethanolate
T=180 - 200°C; im geschlossenen Rohr;
参考文献
Stoermer
Chemische Berichte, 1897 , vol. 30, p. 1706
Justus Liebigs Annalen der Chemie, 1900 , vol. 312, p. 278
Full Text Show Details
Hesse
Chemische Berichte, 1897 , vol. 30, p. 1438
Chemische Berichte, 1898 , vol. 31, p. 601 Anm.
反应条件
poly-phosphoric acid in benzene
3.5 h; Heating;
参考文献
Cody, Wayne Livingston; Edmunds, Jeremy John; Holsworth, Daniel Dale; Powell, Noel Aaron
Patent: US2004/204455 A1, 2004 ;
Location in patent: Page/Page column 18 ;
参考文献
Oezdemir, Ahmet; Turan-Zitouni, Guelhan; Kaplancikli, Zafer Asim; Altintop, Mehlika Dilek
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 2 p. 141 - 146