N-叔丁氧羰基-L-苯丙氨酸苄酯合成路线 (共 22 条)
反应条件
in diethyl ether; chloroform
反应条件
hydrogenchloride in 1,4-dioxane acidolysis;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 14 p. 1497 - 1499
反应条件
sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl (hydroxylimino)cyanoacetate in water; acetonitrile
T=20°C; 2 h;
参考文献
Wang, Yong; Aleiwi, Bilal A.; Wang, Qinghui; Kurosu, Michio
Organic Letters, 2012 , vol. 14, # 18 p. 4910 - 4913,4
Title/Abstract Full Text Show Details
Wang, Yong; Aleiwi, Bilal A.; Wang, Qinghui; Kurosu, Michio
Organic Letters, 2012 , vol. 14, # 18 p. 4910 - 4913
反应条件
potassium carbonate in acetone
Heating / reflux;
参考文献
UNIVERSITY OF WOLLONGONG
Patent: WO2006/74501 A1, 2006 ;
Location in patent: Page/Page column 79 ;
反应条件
4-(N,N-dimethlyamino)pyridine; benzyl alcohol in dichloromethane; water
参考文献
Maeda, Kazuhiro; Sonda, Shuji; Takemoto, Tadahiro; Goto, Tomokazu; Kobayashi, Fujio; Kajii, Masahiko; Komorita, Naruyasu; Hirayama, Fumihiro
Patent: US2003/176486 A1, 2003 ;
反应条件
in toluene
T=80°C; 3 h;
参考文献
Raines, Ronald Thaddeus; Myers, Eddie Leonard
Patent: US2010/125132 A1, 2010 ;
Location in patent: Page/Page column 35 ;
反应条件
tri-i-propoxy lanthanium; 2-(2-methoxy-ethoxy)-ethanol in hexane
T=50°C; Molecular sieve; optical yield given as percent eechemoselective reaction;
参考文献
Hatano, Manabu; Furuya, Yoshiro; Shimmura, Takumi; Moriyama, Katsuhiko; Kamiya, Sho; Maki, Toshikatsu; Ishihara, Kazuaki
Organic Letters, 2011 , vol. 13, # 3 p. 426 - 429
反应条件
triethylamine; N,N,N',N',N''-pentamethylguanidine in dichloromethane
1 h; Ambient temperature;
参考文献
Barcelo, Gerard; Grenouillat, Denis; Senet, Jean-Pierre; Sennyey, Gerard
Tetrahedron, 1990 , vol. 46, # 6 p. 1839 - 1848
反应条件
tetra-(n-butyl)ammonium iodide in water
T=80°C; 8 h; optical yield given as percent ee;
参考文献
Feng, Jie; Liang, Shuai; Chen, Shan-Yong; Zhang, Ji; Fu, Song-Sen; Yu, Xiao-Qi
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1287 - 1292
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
0.333333 h;
参考文献
Takeda; Akiyama; Nakamura; Takizawa; Mizuno; Takayanagi; Harigaya
Synthesis, 1994 , # 10 p. 1063 - 1066