4-(氨基甲基)四氢-2H-吡喃-4-醇盐酸盐合成路线 (共 2 条)
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran; toluene T=0 - 20°C; 4 h; 2: With potassium fluoride; sodium sulfate in tetrahydrofuran; toluene T=0°C; 3: With hydrogenchloride in tetrahydrofuran; ethyl acetate; toluene
参考文献
US2006/94750 A1, ;
Page/Page column 34 ;
US 20060094750 A1
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 4 h; Heating / reflux; 2: With sodium hydroxide; water in tetrahydrofuran 3: With hydrogenchloride in tetrahydrofuran; 1,4-dioxane; diethyl ether; water
参考文献
US2009/76062 A1, ;
Page/Page column 22-23 ;
US 20090076062 A1