乙基(2-甲基苯基)(氧代)乙酸酯合成路线 （共 19 条）
反应条件
boric acid; [Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=60°C; 3 h;
参考文献
Shimizu, Hiroshi; Murakami, Masahiro
Chemical Communications, 2007 , # 27 p. 2855 - 2857
反应条件
1: 1-bromo-2-methyl benzene With magnesium in tetrahydrofuran T=20°C; 1 h; Inert atmosphere; 2: oxalic acid diethyl ester in tetrahydrofuran T=-78°C; 2 h; Inert atmosphere;
参考文献
Hayashi, Masashi; Nakamura, Shuichi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 10 p. 2249 - 2252
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C;
参考文献
Thasana, Nopporn; Prachyawarakorn, Vilailak; Tontoolarug, Sopchok; Ruchirawat, Somsak
Tetrahedron Letters, 2003 , vol. 44, # 5 p. 1019 - 1021
反应条件
magnesium in toluene
反应条件
1: ortho-chlorotoluene With lithium in diethyl ether T=3 - 6°C; 2: With copper (I) cyanide in tetrahydrofuran; diethyl ether T=3 - 6°C; 0.416667 h; Cooling with ice; 3: oxalic acid monoethyl ester chloride in tetrahydrofuran; diethyl ether T=3 - 20°C; 1.25 h;
参考文献
Screttas, Constantinos G.; Steele, Barry R.; Micha-Screttas, Maria; Heropoulos, Georgios A.
Organic Letters, 2012 , vol. 14, # 22 p. 5680 - 5683
反应条件
in diethyl ether T=-78°C; 1 h; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
in tetrahydrofuran; diethyl ether; water
反应条件
chromium(VI) oxide; sulfuric acid
参考文献
Journal of Organic Chemistry, , vol. 73, # 10 p. 3842 - 3847
反应条件
2,2,6,6-tetramethyl-piperidine; 4-nitro-phenol; oxygen; potassium iodide 11.5 h; Electrochemical reaction;
参考文献
Zhang, Zhenlei; Su, Jihu; Zha, Zhenggen; Wang, Zhiyong
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17711 - 17714
反应条件
1: 72 percent / BTAC / CH2Cl2; H2O / 20 °C 2: 64 percent / LDA / tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 5 p. 1019 - 1021
