1,3-二甲氧基-2-硝基苯合成路线 （共 20 条）
反应条件
1: bromine 2: ethanol; tin (II)-chloride; aqueous hydrochloric acid 3: aqueous H2SO4; ethanol / Diazotization View Scheme
参考文献
Lock
Monatshefte fuer Chemie, 1939 , vol. 72, p. 373,374, 375
反应条件
aluminium trichloride; 2-Chloro-2-methylpropane
参考文献
Carpenter et al.
Journal of Organic Chemistry, 1951 , vol. 16, p. 586,606
反应条件
1: acetic acid; tin (II)-chloride; hydrogen chloride 2: Diazotization View Scheme
参考文献
Kauffmann; Franck
Chemische Berichte, 1907 , vol. 40, p. 4006
反应条件
iron; acetic acid in ethanol; water T=90°C;
参考文献
US2007/179164 A1, ;
Page/Page column 56 ;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 372, p. 139
Chemische Berichte, , vol. 40, p. 4006
反应条件
1: acetic acid; tin (II)-chloride; hydrogen chloride
2: Diazotization
3: copper-powder / 130 - 190 °C
View Scheme
参考文献
VanArendonk; Cupery; Adams
Journal of the American Chemical Society, 1933 , vol. 55, p. 4225,4227
参考文献
Vermeulen
Recueil des Travaux Chimiques des Pays-Bas, 1919 , vol. 38, p. 108
参考文献
Kauffmann; Franck
Chemische Berichte, 1906 , vol. 39, p. 2725
反应条件
1: 80 percent / Fe; aq. AcOH / 4 h / 95 °C
2: polyphosphoric acid / 8 h / 80 °C
3: AlCl3 / toluene / 2 h / Heating
View Scheme
参考文献
Larget, Ronan; Lockhart, Brian; Pfeiffer, Bruno; Neudorffer, Anne; Fleury, Maurice-Bernard; Largeron, Martine
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 20 p. 2929 - 2934
反应条件
1: acetic acid; tin (II)-chloride; hydrogen chloride
2: Diazotization
3: copper-powder / 130 - 190 °C
4: aqueous HI
View Scheme
参考文献
VanArendonk; Cupery; Adams
Journal of the American Chemical Society, 1933 , vol. 55, p. 4225,4227
