2,2,2-三氟-n-(三氟乙酰基)乙酰肼合成路线 （共 12 条）
反应条件
N,N-dimethylaniline hydrochloride; trichlorophosphate Heating; Yield given;
参考文献
Barlow, Michael G.; Bell, David; O'Reilly, Neil J.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 293 - 300
参考文献
Reitz, David B.; Finkes, Michael J.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 225 - 230
反应条件
hydrazine hydrate in benzene
27.5 h; Heating;
参考文献
Bell, David; Eltoum, Ahmed O. A.; O'Reilly, Neil J.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1993 , vol. 64, # 1-2 p. 151 - 166
反应条件
trifluoroacetic acid in benzene
参考文献
The University of North Texas
Patent: US2012/118153 A1, 2012 ;
反应条件
hydraziniumdihydrochloride
Heating;
参考文献
Vasiliev, N. V.; Lyashenko, Yu. E.; Patalakha, A. E.; Sokolski, G. A.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 3 p. 227 - 232
反应条件
sodium salt of phosphorous acid in 1,4-dioxane
参考文献
Groth,R.H.
Journal of Organic Chemistry, 1960 , vol. 25, p. 102 - 105
反应条件
in ethanol
dropping of soln. of CF3COOC2H5 in abs. alc. to N2H4 soln. in anhydrous C2H5OH by cooling, stirring at 20°C (12 h); evapn. of C2H5OH, stirring at 20°C (12 h);
参考文献
Young,J.A. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2105 - 2109
反应条件
(i) N2H2, EtOH, (ii) /BRN= 746197/, CF3CO2H; Multistep reaction;
参考文献
Young,J.A. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2105 - 2109
反应条件
in dichloromethane
T=20°C; 14 h;
参考文献
Cesarini, Sara; Colombo, Nicoletta; Pulici, Maurizio; Felder, Eduard R.; Brill, Wolfgang K.-D.
Tetrahedron, 2006 , vol. 62, # 43 p. 10223 - 10236
反应条件
water
Ambient temperature;
参考文献
Barlow, Michael G.; Bell, David; O'Reilly, Neil J.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 293 - 300
