1-甲基-4-(苯磺酰)哌嗪合成路线 （共 7 条）
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile 3 h; Heating;
参考文献
Sabitha, Gowravaram; Subba Reddy; Abraham, Sunny; Yadav
Tetrahedron Letters, 1999 , vol. 40, # 8 p. 1569 - 1570
反应条件
triethylamine in chloroform
T=20°C; 2 h;
参考文献
Kumar Parai, Maloy; Panda, Gautam; Srivastava, Kumkum; Kumar Puri, Sunil
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 2 p. 776 - 781
反应条件
1.1: Mg; I2 / tetrahydrofuran / 1 h / Heating
1.2: SO2 / tetrahydrofuran / 0.5 h / -40 °C
1.3: SO2Cl2 / tetrahydrofuran / -40 - 20 °C
2.1: 84 mg / tetrahydrofuran / 3 h
View Scheme
参考文献
Pandya, Rina; Murashima, Takashi; Tedeschi, Livio; Barrett, Anthony G. M.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8274 - 8276
反应条件
methanol
T=125°C; Erh. des Rktprod. unter vermindertem Druck auf 250grad;
参考文献
Soc. Usines Chim. Rhone-Poulenc
Patent: US2507408 , 1949 ;
反应条件
1: Hydrolysis
2: Na2CO3; ethanol
View Scheme
参考文献
Soc. Usines Chim. Rhone-Poulenc
Patent: US2507408 , 1949 ;
反应条件
2: Hydrolysis
3: Na2CO3; ethanol
View Scheme
参考文献
Soc. Usines Chim. Rhone-Poulenc
Patent: US2507408 , 1949 ;
反应条件
ethanol; sodium carbonate
参考文献
Soc. Usines Chim. Rhone-Poulenc
Patent: US2507408 , 1949 ;
