反应条件
1.1: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / cooling
2.1: trifluoroacetic acid / methanol / cooling
2.2: 89 percent / triethylamine; 4-(dimethylamino)pyridine / tetrahydrofuran / cooling
3.1: 21 percent / (1,3-dimesitylimidazolidin-2-yl)(P(c-Hex)3)(Cl)2Ru=CHC6H5 / CH2Cl2 / 16 h / Heating
4.1: 76 percent / cerium(III) chloride heptahydrate; sodium borohydride / methanol / 3 h / 0 °C
View Scheme
参考文献
Davis, Franklin A.; Wu, Yongzhong
Organic Letters, 2004 , vol. 6, # 8 p. 1269 - 1272