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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66749-96-0
合成路线
（共 9 条）
68-12-2
N,N-二甲基甲酰胺
+
66750-10-5
N-苯氮杂-15-冠-5-醚
→
反应条件
66749-96-0
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate T=0°C; 0.25 h; 2: 13-phenyl-13-aza-1,4,7,10-tetraoxacyclopentadecane T=60°C; 2 h;
参考文献
Oliveira, Elisabete; Baptista, Rosa M.F.; Costa, Susana P. G.; Raposo, M. Manuela M.; Lodeiro, Carlos
Inorganic Chemistry, 2010 , vol. 49, # 23 p. 10847 - 10857
27913-86-6
4-[N,N-双(2-羟乙基)氨基]苯甲醛
+
19249-03-7
三乙二醇二(对甲苯磺酸酯)
→
反应条件
66749-96-0
反应条件
1: 4-lt;N,N-bis(2-hydroxyethyl)aminogt;benzaldehyde With sodium hydride in tetrahydrofuran; mineral oil 0.5 h; RefluxInert atmosphere; 2: triethylene glycol di-p-tosylate in tetrahydrofuran; mineral oil T=70°C; 48 h; Inert atmosphere;
参考文献
Wu, Chia-Shing; Chen, Chiao-Pei; Chen, Yun
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 18 p. 3975 - 3984
37860-51-8
四乙二醇二对甲苯磺酸酯
+
27913-86-6
4-[N,N-双(2-羟乙基)氨基]苯甲醛
→
反应条件
66749-96-0
反应条件
1: 4-lt;N,N-bis(2-hydroxyethyl)aminogt;benzaldehyde With sodium hydride in tetrahydrofuran; mineral oil 0.5 h; Inert atmosphereReflux; 2: tetraethylene glycol di-p-toluenesulfonate in tetrahydrofuran; mineral oil T=70°C; 48 h; Inert atmosphere;
参考文献
Wu, Chia-Shing; Lu, Huai-An; Chen, Chiao-Pei; Guo, Tzung-Fang; Chen, Yun
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 9 p. 1430 - 1439
112-27-6
二缩三乙二醇
→
反应条件
66749-96-0
反应条件
1: sodium hydroxide 2: sodium hydride / tetrahydrofuran 3: trichlorophosphate / N,N-dimethyl-formamide View Scheme
参考文献
Yu, Zhipeng; Duan, Yaya; Cheng, Longhuai; Han, Zhili; Zheng, Zheng; Zhou, Hongping; Wu, Jieying; Tian, Yupeng
Journal of Materials Chemistry, 2012 , vol. 22, # 33 p. 16927 - 16932
120-07-0
N,N-二羟乙基苯胺
→
反应条件
66749-96-0
反应条件
1: 16 percent / NaOH / dioxane / 30 h / Heating 2: 1.) POCl3, 2.) 40percent NaOH / 1.) -10 deg C, 10 min; room temp., 1.5 h; 100 deg C, 4 h, 2.) ice, 1 h View Scheme
参考文献
Dix, Johannes Peter; Voegtle, Fritz
Chemische Berichte, 1980 , vol. 113, # 2 p. 457 - 470
19249-34-4
N,N-二乙酰氧乙基苯胺
→
反应条件
66749-96-0
反应条件
1.1: trichlorophosphate / 1 h / 20 °C / |Cooling with ice 1.2: 12 h / 75 °C 2.1: sodium carbonate / methanol / 20 °C 3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / |Reflux; |Inert atmosphere 3.2: 48 h / 70 °C / |Inert atmosphere View Scheme
参考文献
Wu, Chia-Shing; Chen, Chiao-Pei; Chen, Yun
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 18 p. 3975 - 3984
41313-77-3
4-[双[2-(乙酰氧基)乙基]氨基]苯甲醛
→
反应条件
66749-96-0
反应条件
1.1: sodium carbonate / methanol / 20 °C 2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / |Reflux; |Inert atmosphere 2.2: 48 h / 70 °C / |Inert atmosphere View Scheme
参考文献
Wu, Chia-Shing; Chen, Chiao-Pei; Chen, Yun
Journal of Polymer Science, Part A: Polymer Chemistry, 2013 , vol. 51, # 18 p. 3975 - 3984
19249-03-7
三乙二醇二(对甲苯磺酸酯)
→
反应条件
66749-96-0
反应条件
1: sodium hydride / tetrahydrofuran 2: trichlorophosphate / N,N-dimethyl-formamide View Scheme
参考文献
Yu, Zhipeng; Duan, Yaya; Cheng, Longhuai; Han, Zhili; Zheng, Zheng; Zhou, Hongping; Wu, Jieying; Tian, Yupeng
Journal of Materials Chemistry, 2012 , vol. 22, # 33 p. 16927 - 16932
66750-10-5
N-苯氮杂-15-冠-5-醚
→
反应条件
66749-96-0
反应条件
trichlorophosphate in N,N-dimethyl-formamide
参考文献
Yu, Zhipeng; Duan, Yaya; Cheng, Longhuai; Han, Zhili; Zheng, Zheng; Zhou, Hongping; Wu, Jieying; Tian, Yupeng
Journal of Materials Chemistry, 2012 , vol. 22, # 33 p. 16927 - 16932
