3-(2-硝基-苯基)-丙酸乙酯合成路线 （共 6 条）
参考文献
Gabriel; Zimmermann
Chemische Berichte, 1880 , vol. 13, p. 1680
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide
T=-20 - 70°C; 3 h; Inert atmosphere;
参考文献
Since, Marc; Terme, Thierry; Vanelle, Patrice
Tetrahedron, 2009 , vol. 65, # 31 p. 6128 - 6134
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide
T=-20 - 20°C; 4 h; Inert atmosphere;
参考文献
Since, Marc; Terme, Thierry; Vanelle, Patrice
Tetrahedron, 2009 , vol. 65, # 31 p. 6128 - 6134
反应条件
Pd[(NH3)4]Cl2; C63H112O35; diisopropylamine in water
T=120°C; Heck Reaction; 6 h; Green chemistry; Reagent/catalystTemperature;
参考文献
Al-Maksoud, Walid; Menuel, Stephane; Jahjah, Mohamad; Monflier, Eric; Pinel, Catherine; Djakovitch, Laurent
Applied Catalysis A: General, 2014 , vol. 469, p. 250 - 258
反应条件
sodium tetrahydroborate; palladium on activated charcoal in methanol; water
0.25 h;
参考文献
Hashimoto; Ishizaki; Shudo; Okamoto
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3891 - 3896
反应条件
1: NaBH4 / 10percent Pd-C / methanol; H2O / 0.25 h
2: 33 percent / acetic acid / 0.5 h / Heating
View Scheme
参考文献
Hashimoto; Ishizaki; Shudo; Okamoto
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 11 p. 3891 - 3896
