1: 17 g / NaBH4 / methanol / 1 h / 0 °C 2: 7.1 g / KOAc / dimethylformamide / 18 h / 100 °C View Scheme
参考文献
Green, Michael J.; Tiberi, Robert L.; Friary, Richard; Lutsky, Barry N.; Berkenkoph, Joseph; et al.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 12 p. 1492 - 1495
potassium acetate in N,N-dimethyl-formamide
T=105°C; 5.5 h;
参考文献
Barton, Derek H.R.; Lister-James, John; Hesse, Robert H.; Pechet, Maurice M.; Rozen, Shlomo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1105 - 1110