(2-氯苯基)二苯基甲醇合成路线 (共 17 条)
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in o-xylene T=150°C; 16 h; Inert atmosphere;
参考文献
Bour, James R.; Green, Jacob C.; Winton, Valerie J.; Johnson, Jeffrey B.
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1665 - 1669
反应条件
1: iodine; red phosphorus; aqueous acetic acid 2: pyridine / 200 °C 3: diethyl ether / anschliessend Behandeln mit wss. HCl 4: aqueous HBr; acetic acid View Scheme
参考文献
Bradsher; Smith
Journal of the American Chemical Society, 1943 , vol. 65, p. 451
参考文献
Sumitomo Chemical Company, Limited
Patent: US4216333 A1, 1980 ;
参考文献
Sumitomo Chemical Company, Limited
Patent: US4216333 A1, 1980 ;
反应条件
1: thionyl chloride / Heating 2: triethylamine / acetonitrile / Heating View Scheme
参考文献
Bartroli; Alguero; Boncompte; Forn
Arzneimittel-Forschung/Drug Research, 1992 , vol. 42, # 6 p. 832 - 835
反应条件
1: iodine; red phosphorus; aqueous acetic acid
2: pyridine / 200 °C
3: diethyl ether; benzene / Kochen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit wss. HBr in Essigsaeure
View Scheme
参考文献
Bradsher; Smith
Journal of the American Chemical Society, 1943 , vol. 65, p. 451
反应条件
1: iodine; red phosphorus; aqueous acetic acid
2: pyridine / 200 °C
View Scheme
参考文献
Bradsher; Smith
Journal of the American Chemical Society, 1943 , vol. 65, p. 451