反应条件
1: 92 percent / N-bromoacetamide / acetic acid / 1.5 h / Ambient temperature
2: 84 percent / N-bromoacetamide, α,α-azoisobutyronitrile / CCl4 / 0.75 h / Heating
3: 1) NaOMe, 2) TFA / 1) 0 deg C, 2 h then 4 deg C, overnight, 2) CDCl3
View Scheme
参考文献
Agarwal, Shiv K.; Boyd, Derek R.; Dunlop, Robert; Jennings, W. Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 3013 - 3018
