反应条件
1: 171 mg / BCl3 / CH2Cl2 / 5 h / Ambient temperature
2: pyridine / 3 h / 90 °C
3: 1.) Br2, 2.) H2O / 1.) CCl4, reflux, 15 min, irradiation, 2.) dioxan, reflux, 4.5 h
4: 210 mg / pyridinium chlorochromate / CH2Cl2 / 3 h
5: 67 mg / LiI / hexamethylphosphoric acid triamide / 40 h / Heating
View Scheme
参考文献
Sala, Tony; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 877 - 882
