2,3-二氢-4,7-二甲基-1H-茚合成路线 （共 13 条）
反应条件
hydrogenchloride; acetic acid; zinc in water
参考文献
ICI Australia Limited
Patent: US4952722 A1, 1990 ;
反应条件
iodine; triethylamine in diethyl ether
T=25°C;
参考文献
Jung, Michael E.; Hatfield, Gregory L.
Tetrahedron Letters, 1982 , vol. 23, # 39 p. 3991 - 3994
反应条件
hydrogenchloride; Zn–Hg amalgam
参考文献
Avila, David V.; Davies, Alwyn G.; Li, Elizabeth R.; Ng, Kai M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 3 p. 355 - 362
反应条件
hydrogen; platinum(IV) oxide in acetic acid
参考文献
Murray,R.D.H. et al.
Tetrahedron, 1962 , vol. 18, p. 55 - 60
反应条件
triphenylphosphine in tetrachloromethane
参考文献
Jung, Michael E.; Hatfield, Gregory L.
Tetrahedron Letters, 1982 , vol. 23, # 39 p. 3991 - 3994
反应条件
1: LiAlH4
2: H2 / PtO2 / acetic acid
View Scheme
参考文献
Murray,R.D.H. et al.
Tetrahedron, 1962 , vol. 18, p. 55 - 60
反应条件
tetrachloromethane; triphenylphosphine
10 h; Heating;
参考文献
Jung, Michael E.; Hatfield, Gregory L.
Tetrahedron Letters, 1983 , vol. 24, # 31 p. 3175 - 3178
反应条件
potassium tert-butylate; iodine; triethylamine
1.) ether, 25 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jung, Michael E.; Hatfield, Gregory L.
Tetrahedron Letters, 1983 , vol. 24, # 31 p. 3175 - 3178
反应条件
1: xylene / Erwaermen des Reaktionsprodukts mit aethanol. Kalilauge und Erhitzen der erhaltenen <2.5-Dimethyl-benzyl>-malonsaeure
2: benzene; thionyl chloride
3: AlCl3; petroleum ether
4: amalgamated zinc; aqueous HCl
View Scheme
参考文献
Plattner; Wyss
Helvetica Chimica Acta, 1941 , vol. 24, p. 483,491
反应条件
1: benzene; thionyl chloride
2: AlCl3; petroleum ether
3: amalgamated zinc; aqueous HCl
View Scheme
参考文献
Plattner; Wyss
Helvetica Chimica Acta, 1941 , vol. 24, p. 483,491
