2-[(2-氯苯甲酰基)氨基]乙酸乙酯合成路线 （共 4 条）
反应条件
sodium hydrogencarbonate
参考文献
DE2745222 , ;
Chem.Abstr., , vol. 89, # 42840
反应条件
1: SOCl2, DMF / toluene / 0.5 h / 60 - 70 °C 2: K2CO3 / H2O; toluene / -5 - 5 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 28, # 7 p. 2045 - 2051
反应条件
1,1'-carbonyldiimidazole 1) DMF, 0 deg C -> room temperature, 20 min, 2) DMF, room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1539 - 1545
反应条件
water; sodium hydroxide in 2-methyl tetrahydrofuran T=25 - 28°C; 1 h;
参考文献
Chavez, Flavio; Kennedy, Nicole; Rawalpally, Thimma; Williamson, R. Thomas; Cleary, Thomas
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 579 - 584
