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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
668268-67-5
合成路线
（共 9 条）
2402-78-0
2,6-二氯吡啶
→
反应条件
668268-67-5
反应条件
1: CF3COOH; aq. H2O2 / 6.5 h / Heating 2: HNO3; H2SO4 / 160 °C 3: AcOH; Fe / Heating 4: HNO3; H2SO4 / 20 °C 5: H2SO4 / 100 °C 6: 51 percent / Fe / 2 h / Heating 7: aq. NaOH / Heating 8: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
2587-02-2
4-氨基-2,6-二氯吡啶
→
反应条件
668268-67-5
反应条件
1: HNO3; H2SO4 / 20 °C 2: H2SO4 / 100 °C 3: 51 percent / Fe / 2 h / Heating 4: aq. NaOH / Heating 5: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
2587-00-0
4-二甲胺基吡啶N-氧化物
→
反应条件
668268-67-5
反应条件
1: HNO3; H2SO4 / 160 °C 2: AcOH; Fe / Heating 3: HNO3; H2SO4 / 20 °C 4: H2SO4 / 100 °C 5: 51 percent / Fe / 2 h / Heating 6: aq. NaOH / Heating 7: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
2587-03-3
→
反应条件
668268-67-5
反应条件
1: H2SO4 / 100 °C 2: 51 percent / Fe / 2 h / Heating 3: aq. NaOH / Heating 4: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
2897-43-0
4-氨基-2,6-二氯-3-硝基吡啶嘧啶
→
反应条件
668268-67-5
反应条件
1: 51 percent / Fe / 2 h / Heating 2: aq. NaOH / Heating 3: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
25194-01-8
2,6-二氯-4-硝基吡啶
→
反应条件
668268-67-5
反应条件
1: AcOH; Fe / Heating 2: HNO3; H2SO4 / 20 °C 3: H2SO4 / 100 °C 4: 51 percent / Fe / 2 h / Heating 5: aq. NaOH / Heating 6: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
668268-66-4
→
反应条件
668268-67-5
反应条件
1: aq. NaOH / Heating 2: 38 percent / 72 h / Heating View Scheme
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
64-18-6
甲酸
+
101079-63-4
2,6-二氯吡啶-3,4-二胺
→
反应条件
668268-67-5
反应条件
72 h; Heating;
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
668268-67-5
→
反应条件
668268-68-6
4,6-二氯-1H-咪唑并[4,5-c]吡啶-2(3h)-酮
反应条件
potassium hydroxide Heating;
参考文献
Seley, Katherine L.; O'Daniel, Peter I.; Salima, Samer
Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 12 p. 2133 - 2144
