3-甲基-4-苯基-1-丁烯合成路线 （共 61 条）
反应条件
Cs/Na/K alloy multistep reaction: 1.) THF, -75 deg C, 2 h, rate of cleavage relative to bibenzyl; Product distributionRate constant;
参考文献
Grovenstein, Erling; Bhatti, Amjad M.; Quest, Dean E.; Sengupta, Dibyendu; VanDerveer, Don
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6290 - 6299
反应条件
oxygen; cobalt(II) 2,4-pentanedionate in isopropyl alcohol T=75°C; 1 h;
参考文献
Chemistry Letters, , p. 449 - 452
反应条件
oxygen; cobalt(II) 2,4-pentanedionate in isopropyl alcohol T=75°C; 1 h;
参考文献
Chemistry Letters, , p. 449 - 452
反应条件
sodium hydrogen telluride in ethanol 72 h; Heating; Yield given;
参考文献
Tetrahedron, , vol. 46, # 15 p. 5273 - 5284
反应条件
sodium hydrogen telluride in ethanol 72 h; Heating; Product distributionMechanism;
参考文献
Tetrahedron Letters, , vol. 31, # 1 p. 93 - 96
反应条件
1: Methyltriphenylphosphonium bromide With sodium hexamethyldisilazane in tetrahydrofuran
T=25°C; Wittig reaction; 1 h;
2: 4-phenyl-butan-2-one in tetrahydrofuran
T=25°C; Wittig reaction;
参考文献
Lebel, Helene; Guay, Danielle; Paquet, Valerie; Huard, Kim
Organic Letters, 2004 , vol. 6, # 18 p. 3047 - 3050
反应条件
triphenylphosphine; isopropyl alcohol; Wilkinson's catalyst in 1,4-dioxane
T=60°C;
参考文献
Lebel, Helene; Guay, Danielle; Paquet, Valerie; Huard, Kim
Organic Letters, 2004 , vol. 6, # 18 p. 3047 - 3050
反应条件
N,N,N',N,-tetramethylethylenediamine; iron(III) chloride in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Guerinot, Amandine; Reymond, Sebastien; Cossy, Janine
Angewandte Chemie - International Edition, 2007 , vol. 46, # 34 p. 6521 - 6524
反应条件
titanium tetrachloride; zinc; PbCl2 in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Takai, Kazuhiko; Kakiuchi, Tadahiro; Kataoka, Yasutaka; Utimoto, Kiitiro
Journal of Organic Chemistry, 1994 , vol. 59, # 10 p. 2668 - 2670
反应条件
1: 3-chloro-2-methyl-propene With magnesium in tetrahydrofuran
2: benzyl bromide in tetrahydrofuran
Grignard coupling; 3 h; Heating;
参考文献
Hoffmann, Reinhard W.; Haeberlin, Eckart; Rohde, Thorsten
Synthesis, 2002 , # 2 p. 207 - 212
