1-[2,4-双(苯甲酰氧基)苯基]乙酮合成路线 （共 13 条）
反应条件
1: 90 percent / Br2 / CCl4 / Heating
2: toluene / Heating
3: 1.) 47percent HBr; 2.) aq.Na2CO3 / 1.) 100 deg C
4: 2.) 0.5N NaOH / 1.) pyridine, 3 h, 60 deg C; 2.) 50 deg C, 1 h
View Scheme
参考文献
Le Floc'H, Yves; Lefeuvre, Martine
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2751 - 2752
反应条件
1: With sodium hydroxide in dimethyl sulfoxide
Baker-Venkataraman transformation; 0.166667 h;
2: With water in dimethyl sulfoxide
Cooling;
参考文献
Sheikh, Javed; Parvez, Ali; Juneja, Harjeet; Ingle, Vishwas; Chohan, Zahid; Youssoufi, Moulay; Ben Hadda, Taibi
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 4 p. 1390 - 1399
反应条件
1: potassium carbonate / acetone / Heating
2: potassium carbonate / H2O
View Scheme
参考文献
Baker et al.
Journal of the Chemical Society, 1952 , p. 1505
