11-叠氮基-1-十一烷硫醇合成路线 （共 6 条）
反应条件
1: With thiourea in ethanol
T=80°C; 16 h;
2: With sodium hydroxide in ethanol; water
T=20°C; 0.0833333 h; Further stages.;
参考文献
Lin, Yu-Yun; Tsai, Shih-Chung; Yu, Shuchun Joyce
Journal of Organic Chemistry, 2008 , vol. 73, # 13 p. 4920 - 4928
反应条件
1: With thiourea in ethanol
T=80°C; 10 h; Inert atmosphere;
2: With sodium hydroxide in ethanol
T=100°C; 4 h;
3: With hydrogenchloride in ethanol; water
T=20°C;
参考文献
Nguyen, Dao M.; Frazer, Andrew; Rodriguez, Luis; Belfield, Kevin D.
Chemistry of Materials, 2010 , vol. 22, # 11 p. 3472 - 3481
反应条件
hydrogenchloride in methanol
Inert atmosphereReflux;
参考文献
Bandyopadhyay, Sabyasachi; Mukherjee, Sohini; Dey, Abhishek
RSC Advances, 2013 , vol. 3, # 38 p. 17174 - 17187
反应条件
1.1: sodium azide / acetonitrile / 20 h / 80 °C / Inert atmosphere
2.1: pyridine / 3.33 h / 5 °C / Inert atmosphere
3.1: thiourea / ethanol / 10 h / 80 °C / Inert atmosphere
3.2: 4 h / 100 °C
3.3: 20 °C
View Scheme
参考文献
Nguyen, Dao M.; Frazer, Andrew; Rodriguez, Luis; Belfield, Kevin D.
Chemistry of Materials, 2010 , vol. 22, # 11 p. 3472 - 3481
反应条件
1.1: trifluoroacetic anhydride / tetrahydrofuran / Inert atmosphere
1.2: Inert atmosphere
1.3: Inert atmosphere
2.1: thiourea / ethanol / Inert atmosphere
2.2: Inert atmosphere
2.3: Inert atmosphere
View Scheme
参考文献
Bian, Shudan; Schesing, Kevin B.; Braunschweig, Adam B.
Chemical Communications, 2012 , vol. 48, # 41 p. 4995 - 4997
反应条件
1: methanol / |Reflux; |Inert atmosphere
2: hydrogenchloride / methanol / |Inert atmosphere; |Reflux
View Scheme
参考文献
Bandyopadhyay, Sabyasachi; Mukherjee, Sohini; Dey, Abhishek
RSC Advances, 2013 , vol. 3, # 38 p. 17174 - 17187
