反应条件
1: 2-(trimethylsilyl)-1,3-dithiane With n-butyllithium in diethyl ether; hexane
T=-30°C;
2: With copper(I) bromide dimethylsulfide complex in diethyl ether; hexane
T=-60°C; 1 h;
3: 1-bromopinacolone in diethyl ether; hexane
T=-60 - -30°C;
参考文献
Claessen, Rolf U.; Kornilov, Andrei M.; Banger, Kulbinder K.; Ngo, Silvana C.; Higashiya, Seiichiro; Wells, Christopher C.; Dikarev, Evgeny V.; Toscano, Paul J.; Welch, John T.
Journal of Organometallic Chemistry, 2004 , vol. 689, # 1 p. 71 - 81
